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NR9-1500PY process recipe

NR9-1500PY is Futurrex's negative-tone 365 nm lift-off resist, coating ~1.2–3.0 µm with an undercut sidewall tunable by exposure dose. It needs 190 mJ/cm² at 365 nm (1 µm film), develops in aqueous RD6 and strips in RR5.

https://nanyte.com/photoresists/nr9-1500py · last updated 2026-07-26

At a glance
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Manufacturer
Futurrex, Inc.
Tone
negative
Thickness
1.2–3 µm
Exposure dose
190 mJ/cm² at 365 nm
Developer
Resist Developer RD6
Applications
Lift-off · Etch mask

Cross-checked — two independent extractions agree on the spin curve and the single-value figures.

The exposed resist stays after development; the unexposed film dissolves. Schematic cross-sections for NR9-1500PY — feature width, film aspect ratio and sidewall angle are illustrative, not to scale.
01 / Coating

Spin coating

Spin curve for NR9-1500PY: film thickness in µm against spin speed in rpm.1.01.52.02.53.03.51k2k3k4k5kSPIN SPEED (rpm)THICKNESS (µm)
Data points
NR9-1500PY — film thickness (µm) by spin speed (rpm)
Seriesrpmµm
NR9-1500PY8003.0
10002.7
20001.9
30001.5
40001.3
50001.2

Values are the manufacturer’s starting points, not a guarantee — characterize on your own tool.

numeric table 'Film thickness after 150°C hotplate bake for 60 s. / Coating spin speed, 40 s spin (rpm): (nm)', p.1 of Futurrex NR9-1500PY Technical Information. The datasheet publishes each point as an nm RANGE, not a single value (e.g. 800 rpm -> 2850-3150 nm); each point above is the exact midpoint of that stated range (every range is symmetric, approx. nominal +/-5%), converted nm->um. Raw ranges: 800rpm=2850-3150nm, 1000rpm=2565-2835nm, 2000rpm=1805-1995nm, 3000rpm=1425-1575nm, 4000rpm=1235-1365nm, 5000rpm=1140-1260nm. The 3000 rpm midpoint (1500 nm = 1.5 um) matches the '1500' in the product name NR9-1500PY, corroborating the midpoint reading.

Redrawn from the manufacturer's published data — hover to read between points, click to pin.
  • Spin coating is at a selected speed for 40 s (Processing step 1).
  • Edge Bead Remover EBR2 is dispensed simultaneously onto top and bottom surfaces through nozzles 0.5-1.0 cm from the substrate edge, starting as soon as edge bead forms (3-5 s after resist dispense ends) and stopping 5 s before spin cycle completion (Processing step 2).
  • Bake times throughout this datasheet assume a good thermal conductor substrate (Si, GaAs); the datasheet instructs multiplying bake times by 3.5 for poor thermal conductors such as glass.
Adhesion
HMDS not required — Not addressed in this datasheet.
02 / Bake

Soft bake

Soft bake
150 °C · 60 s · hotplate
Notes
Applies to good thermal conductors (Si, GaAs, etc.); bake times must be multiplied by 3.5 for poor thermal conductors such as glass (no explicit alternate schedule given for this SKU, unlike NR71-3000P's dual schedule).

SOURCE: Processing step 3, p.2; corroborated by Properties table heading, p.1

03 / Exposure

Exposure dose

The manufacturer publishes 190 mJ/cm² at 365 nm. Dose scales with film thickness and depends on your optics, so treat it as a starting point and run a dose array.

Dose at 365 nm
190 mJ/cm²
Dose at 405 nm
Not published — characterize on-tool
As published
190 mJ/cm² at 365 nm is the only exposure figure Futurrex prints for this resist, and it is normalized to a 1 µm film — there is no h-line number and nothing for a thicker coat.
Post-exposure bake
100 °C · 60 s

SOURCE: Properties, p.1

04 / Development

Development

Developer
Resist Developer RD6
Time
12 s
Rinse
Deionized water rinse until water resistivity reaches prescribed limit (Processing step 7).
Developer family
TMAH-based

Not published for this resist: Dilution, Method — characterize on-tool.

SOURCE: Processing steps 6-7, p.2

05 / Post-processing

Hard bake, etch & strip

Etch resistance
"Superior selectivity in RIE process" (Description, p.1).
Stripper
Resist Remover RR5 at room temperature (Processing step 9, p.2).
Storage
"Guaranteed shelf life at 25°C storage (years) 3" (Properties, p.1); "shelf life exceeding 3 years at room temperature storage" (Description, p.1).

Not published for this resist: Hard bake, Descum — characterize on-tool.

06 / Applications

Where it's used

Practical notes from the datasheet

NR9-1500PY is Futurrex's negative-tone, 365 nm lift-off resist, formulated in cyclohexanone and developed in the basic aqueous RD6 developer; degree of undercut is tuned by exposure dose (per the datasheet, 'easy adjustment of the degree of resist undercut as a function of exposure energy') as well as by extending development time via RD6/water dilution. The product code encodes its reference film thickness: '1500' corresponds to the 3000 rpm/40 s coating point (1425-1575 nm, midpoint 1.5 µm) in the published spin table. Bake times given here (150°C softbake, 100°C PEB, both 60 s) assume a substrate that conducts heat well (silicon, GaAs); the datasheet explicitly instructs multiplying bake times by 3.5 on poor thermal conductors such as glass — a detail easy to miss when porting a Si recipe to a transparent substrate. Sensitivity is published as 190 mJ/cm² at 365 nm normalized to a 1 µm-thick film rather than as an absolute dose for whatever process thickness is actually chosen, and no h-line (405 nm) dose is given.

07 / Troubleshooting

Troubleshooting

Common failure modes for NR9-1500PY, answered from the manufacturer's datasheet and application notes. These are starting points — your substrate, tooling and environment shift the specifics, so calibrate on-tool.

How do I control the lift-off undercut with NR9-1500PY?

NR9-1500PY is a negative-tone resist whose degree of undercut is tuned by exposure energy — the datasheet's stated advantage is 'easy adjustment of the degree of resist undercut as a function of exposure energy.' The undercut can also be opened up by extending development. Process is soft bake 150°C/60 s, expose at 365 nm, PEB 100°C/60 s, develop in RD6, then strip in RR5.

SOURCE: Futurrex NR9-1500PY Technical Information — Description, p.1, and Processing steps 3–9, p.2

What is the develop time for NR9-1500PY, and how do I extend it?

The standard example is 12 s in Resist Developer RD6 for a 1.5 µm film, including overdevelopment, by spray or immersion, followed by a DI-water rinse to the prescribed resistivity. To slow the develop down to a 60 s process, the datasheet specifies diluting RD6 with water 3:1 — a distinct, slower develop rather than simply running the neat developer longer.

SOURCE: Futurrex NR9-1500PY Technical Information — Processing steps 6–7, p.2

What exposure dose does NR9-1500PY need at 365 nm?

Sensitivity is published as 190 mJ/cm² at 365 nm, explicitly normalized to a 1 µm-thick film — not an absolute dose for an arbitrary process thickness, and the datasheet gives no scaling formula, so treat it as a starting point and calibrate for your film. Exposure must be at 365 nm; no h-line (405 nm) dose is published.

SOURCE: Futurrex NR9-1500PY Technical Information — Properties, p.1

Do I change the bake for NR9-1500PY on glass or other poor thermal conductors?

Yes. The 150°C/60 s soft bake and 100°C/60 s PEB assume a good thermal conductor such as silicon or GaAs; on a poor thermal conductor such as glass the datasheet instructs multiplying the bake times by 3.5 — easy to miss when porting a silicon recipe to a transparent substrate.

SOURCE: Futurrex NR9-1500PY Technical Information — Processing steps 3 & 5, p.2

08 / Sources

Sources & disclaimer

Research using this resist
  1. Karnati et al.. Micromachining on and of Transparent Polymers for Patterning Electrodes and Growing Electrically Active Cells for Biosensor Applications. Micromachines (2017). doi:10.3390/mi8080250
    NR9 lift-off gold MEAs on flexible PEN for biosensors

Manufacturer datasheet values are starting points; optimal parameters depend on your substrate, equipment and environment. Product names and trademarks belong to their respective owners. NANYTE is not affiliated with the manufacturers listed. Last updated 2026-07-26.

Cite this recipe

NANYTE. "NR9-1500PY process recipe." NANYTE Photoresist Library. https://nanyte.com/photoresists/nr9-1500py. Accessed 2026-07-26.

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Expose it at 365 and 405 nm

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